Ndfeb hydrogen decrepitation.jpeg

The treatment starts with a hydrogen decrepitation (HD) process to transform the as extracted waste magnets into an almost fully demagnetized powder for an easy separation of the magnetic fraction from the rest of the materials (corrosion protection layers or, depending on the device, the assembly where the magnet was fixed into) [6]. ….

A high performance sintered NdFeB magnet with N52 was prepared by strip casting, hydrogen decrepitation, jet milling, rubber isostatic pressing with impulse magnetic field and vibrating. The structure of the magnet was investigated by XRD, optical microscope, TEM and SEM, and its demagnetization curve was tested by magnetograph. The results …magnets. The thermal and mechanical impact of the hydrogen decrepitation process was assessed during hydrogen processing. For all forms of sintered NdFeB scrap the surface condition of the magnets is important as oxidation has been shown to inhibit the onset of the hydrogen decrepitation process. In this

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Dec 20, 2020 · Extraction of NdFeB from rotors using hydrogen. Seven semi-embedded rotors and non-embedded rotors were processed separately in two experiments. All the magnets in individual slots were scored in concentric circles using an angle grinder to provide a fresh surface for the hydrogen, as shown in Fig. 3, 15–30 min before being loaded into the ... Hydrogen decrepitation (HD) is based on the selective synthesis of neodymium hydrides though the reaction of hydrogen gas with neodymium located in the Nd-Fe-B magnet. HD process was originally designed and patented by Harris et al. (1979) as a way to break down SmCo and Sm 2(Co,Fe,Cu,Zr) alloys. 5 17. Another example of the coercivity recovery in crushed NdFeB-type sintered magnets was made by adding the DyF 3 salt [8]. Furthermore, the production of anisotropic RE–Fe–B–Cu powders have also been produced by hydrogen decrepitation of hot deformed ingots [9] followed by degassing.

Keywords: Finite difference method; Kinetics; Hydrogen decrepitation; NdFeB alloys; Diffusion 1. Introduction Sv (V ) expansion due to decrepitation results in a five orders of magnitude higher rate of hydrogen diffusion into The most popular recent application of hydrogen in the Nd–Fe–B alloy than into a theoretical bulk sample of that ...Abstract: Hydrogen decrepitation (HD) is an effective and environmentally friendly technique for recycling of neodymium-iron-boron (NdFeB) magnets. During the HD process, the NdFeB breaksSemantic Scholar extracted view of "Possible methods of recycling NdFeB-type sintered magnets using the HD/degassing process" by M. Zakotnik et al. ... The purpose of this thesis was to study the Hydrogen Decrepitation (HD) process as a way to recycle waste scraps of Nd-Fe-B sintered magnets into highly coercitive and anisotropic …The processing and characterisation of recycled NdFeB-type sintered magnets. M. Degri. Materials Science, Engineering. 2014. A study of the processing and characterisation of sintered NdFeB magnets made from recycled feed stock was undertaken. Initially the hydrogen decrepitated (HD) powder was investigated using two…. Expand. The Hydrogen Decrepitation process (HD) is used as an alternative method of powder preparation in the manufacturing process of sintered Nd Fe B magnets [ 1]. During the HD process a NdFeB-type material is hydrogenated by gaseous hydrogen at atmospheric (or elevated) pressure at room (or elevated) temperature.

Abstract: Hydrogen decrepitation (HD) is an effective and environmentally friendly technique for recycling of neodymium-iron-boron (NdFeB) magnets. During the …The hydrogen decrepitation (HD) behaviors of various forms of the permanent magnet alloy Nd{sub 16}Fe{sub 76}B{sub 8} and stoichiometric composition Nd{sub 11.8}Fe{sub 82.3}B{sub 5.9} have been investigated to provide background information on the production of sintered magnets by the HD process. ... The procedure …Jan 1, 2018 · High-temperature demagnetization can, however, cause melting of components, e.g., plastics, glue, etc. Hydrogen decrepitation (Table 8.3), a more efficient alternative, has been suggested for processing of HDDs [34], [35]. The NdFeB magnets absorb hydrogen, expanding in volume with about 5%, which causes breaking into coarse granules or powder. ….

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Michihide Nakamura, Masashi Matsuura, Nobuki Tezuka, Satoshi Sugimoto, Yasuhiro Une, Hirokazu Kubo, Masato Sagawa; Preparation of ultrafine jet-milled powders for Nd-Fe-B sintered magnets using hydrogenation–disproportionation–desorption–recombination and hydrogen …Abstract. Some fully dense, sintered NdFeB-type magnets (employed in VCM disc drives) have been subjected to a recycling process using the hydrogen decrepitation (HD) process. After a brief milling treatment, the powder was aligned, pressed and re-sintered and this procedure was repeated four times with a progressive fall in the density …Hydrogen decrepitation (HD) of Nd-Fe-B cast alloys is widely used in the processing of sintered magnets. The oxidation resistance under air of alloy powder …

Hydrogen decrepitation of Nd-Fe-B type magnet alloys is a two stage process. Firstly, the hydrogen reacts with the Nd-rich phase at or close to room …The U.S. Department of Energy's Office of Scientific and Technical InformationMar 1, 2019 · Fig. 1 shows the hydrogen decrepitation curves of Nd-Fe-B SC and SM at 288 K with different initial hydrogen pressure. Under the initial hydrogen pressure of 0.1–1 Mpa, the HD process composes of four stages of magnets surface activation, slow hydrogenation of Nd-rich grain boundary phase, quick hydrogenation of Nd 2 Fe 14 B main phase grains, and slow hydrogenation of inner part of the magnets.

offerta ondaflex So exposure at LOW temperature to hydrogen leads the NdFeB pieces to react via intergranular fracturation (decrepitation), the mass of Nd2Fe14B grains forminfg a metal hydride with max ...Sep 7, 2022 · We report investigations on the processing by Spark Plasma Sintering (SPS) of RE2Fe14B (RE = Nd, Pr…) powders obtained by hydrogen decrepitation of decommissioned magnets and the magnetic properties of the consolidated magnets. First experiments have been carried out with a commercial powder to make clear the mechanisms occurring during the powder densification. The magnetic properties of ... bluey motherhj For the second type, three popular techniques, hydrogen decrepitation (HD), HDDR, and MS are applied to produce magnetic powders with the waste magnets. Note that the resultant powders prepared from the three techniques are single crystal powders, textured polycrystalline powders, and random aligned polycrystalline powders, respectively. ... tpandw railroad Fully dense sintered NdFeB-type magnets have been subjected to the hydrogen decrepitation (HD) process. The resultant powder has been subsequently processed in one of two ways in order to produce ...The Hydrogen Decrepitation and the Hydrogen Disproportionation Desorption Recombination processes for the preparation and the recycling of the two industrially produced phases of SmCo alloys, SmCo5 and Sm2Co17, are reviewed. The effects of the chemical composition, the microstructure, the exposure time, the hydrogen … test2peg leg petehow to find person A combination of hydrogen decrepitation (HD) and jet milling (JM) has been used to produce powder for the processing of permanent magnets. The procedure has proved to be very successful for both Nd-Fe-B (Neomax) alloys and the ND-Dy-Fe-Nb-B high coercivity alloys. The magnets produced by the HD/JM process showed excellent coercivities when … university of texas at arlington masterpercent27s programs Hydrogen decrepitation (HD) is based on the selective synthesis of neodymium hydrides though the reaction of hydrogen gas with neodymium located in the Nd-Fe-B magnet. HD process was originally designed and patented by Harris et al. (1979) as a way to break down SmCo and Sm 2(Co,Fe,Cu,Zr) alloys. 5 17. avestevens 22 410 over under priceopercent27reillypercent27s choctaw A bulk ingot of a Nd-Fe-B alloy has been powdered by a combination of hydrogen decrepitation and attritor milling. The powder was aligned and pressed in the hydrided condition and the green compact sintered at 1080‡ C for 1 h after an appropriate heating rate. Excellent densities were achieved after this procedure and the magnets produced …